storage use

WRI-HTP (FR7.1)

Experimental High Temperature - High Pressure Rock/Fluid interactions facilities

Operated by
CNRS
Centre national de la recherche scientifique
1A Rue de la Ferollerie, 45100, Orléans, France
CCUS Technologies
storage
Pressure/injection, Migration, Reactivity/mineralisation
use
CO2 Conversion to Solid Carbonates
Research Fields
Fluid dynamics, Chemistry/Geochemistry, Geology/Geophysics, Material science, Physical processes, Thermodynamics
Scale of Facility
Lab Scale
Forms of Access
In Person
Other CCUS Projects
ANR

2011 - 2015

FluxHyd

Labex-Equipex

2011-2024

Voltaire

This facility provides state-of-the-art equipments for the experimental study of hydrothermal processes (i.e. 0 to 500 bars and up to 300-400°C). The facility is equipped with 2 Dixon-Seyfried rocking autoclaves which are operating with titanium bags and are equipped with a sampling port for gas and fluid analysis; as well as several cold-seal autoclaves working with golden capsules up to 3kbar and 850°C for hydrothermal synthesis.

The facility also has 2 permeameters (flow-through devices) allowing the injection of fluids through a rock core (diam 5.6mm, length few cm) up to 500 bar and 400°C. This set up allows the investigation of reactive transport in hydrothermal conditions, and in particular to study the in-situ carbonation of ultramafic rocks.

Scientific Environment

The facility is incorporated in the experimental facilities of the laboratory offering experiments from high temperatures and pressures (GPa, several thousands degrees), to the hydrothermal conditions described here. The facility also benefits from a dedicated workshop for the repairs as well as the development of new functionalities. Finally, the laboratory also offers state-of-the-art analytical facilities, both for the solid and the fluid (XRD, SEM, TEM, gas and liquid chromatography and ICP-MS).

State of the Art, Uniqueness & Specific Advantages

The permeameters are unique as they offer a range of working pressure and temperature higher than similar facilities. The combination of batch autoclaves and reactive transport experiments also allows for the consistent investigation of hydrothermal processes, both in terms of mineralogy and mineral synthesis but also in terms of transport processes and hydrochemical feedbacks.

Quality Control / Quality Assurance (QA)

Activities / Tests / Data are

Controlled: ISO9001

Facility Availability

Unit of Access (UA)

Week

Availability per Year (in UA)

12 weeks

Duration of a Typical Access (Average) and Number of External Users Expected for that Access

Average access depends on the type of rock and chemical reactions considered. Experiments can last from a few days to several months.Presence of external users is required for at least 1 week to prepare the experiment (starting) and a couple of days to stop it.

Operational or Other Constraints

Specific Risks

High pressure and high temperature systems.

Legal Issues

n/a